1. Distillation Operation

Henry Z. Kister, «Distillation Operation» McGraw-Hill Professional
ISBN: 007034910X | 1 edition (January 1, 1990) | 729 pages | PDF | 31.3 Mb
There are many books that discuss distillation, but there is only one that concentrates on giving readers practical guidelines for operation, troubleshooting and control. This is that book. Its contents revolves around over 300 actual case histories of distillation problems that occurred in the past. Each problem and its solution are briefly described, and the lessons learned are molded into the practical guidelines that make up the book. Carefully focused, the book shows you how over 90% of all column malfunctions occurred in the past, how they were solved, and how to prevent them in the future. Starting with column internals and their malfunctions, it progresses to installation, commissioning, startup and normal operation before surveying the auxiliary system and the column automatic controls--how they should be, how they can go wrong, and how you can repair them. This book offers the best available compendium of Do's and Don'ts, good practices, and guidelines for trouble-free design, operation and troubleshooting for inlets and outlets; distributors; avoiding tray damage; installation; commissioning and startup techniques; column flood and efficiency testing; pressure, temperature and boilup control; and many more.
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2. Distillation Operation
By Henry Z. Kister
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3. Ola Norrman - Home Distillation Handbook

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4.
Design of Distillation Column Control Systems
Design of Distillation Column Control Systems
576 pages | Publisher: Butterworth-Heinemann (December 1, 1985) | Language: English | ISBN:
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Book Description
A distillation column is both multivariable and nonlinear - and it consumes immense quantities of energy. Yet, despite the desigh challenges it presents, it is still the most popular unit operation for refining in industrial plants today. Much has been published on the subject of distillation column design, but much remains to be explained. That is why this book is unique. In a departure from the more traditional empirical and theoretical approaches, it introduced the reader to the practical realm, by presenting quantitative design techniques that have been demonstrated to be useful and valid over the course of hundreds of actual applications.
The book is divided into three main parts. Part I, an introduction, presents an industrial perspective of control objectives. It discusses briefly the relationship between column design features and column controllability. It thus provides a short refresher course for chemical engineers and background for those trained in other branches of engineering. Part II, Concepts and Configurations, discusses column overhead and base arrangements, typical control schemes, and some hardware considerations. Part III is dedicated to quantitative design. Mathematical models are presented for pressure and differential pressure controls, liquid level control, and composition control of binary distillation.
Emphasis on topics of primary interest to the control engineer
Essentially nonmathematical treatment
Ideal for those involved in troubleshooting existing columns as well to design engineers
🔒 Bấm Cảm ơn hoặc Trả lời để xem Link5. I. M. Mujtaba, «Batch Distillation: Design and Operation»
I. M. Mujtaba, «Batch Distillation: Design and Operation»
Imperial College Press | ISBN: 186094437X | 2004 Year | 416 Pages| PDF | 13,9 Mb
Description:
The batch distillation process has existed for many centuries. It is perhaps the oldest technology for separating or purifying liquid mixtures and is the most frequently used separation method in batch processes. In the last 25 years, with continuous development of faster computers and sophisticated numerical methods, there have been many published works using detailed mathematical models with rigorous physical property calculations and advanced optimisation techniques to address several important issues, such as selection of column configurations, design, operation, off-cut recycling, use of batch distillation in reactive and extractive modes, etc.
Batch Distillation: Design and Operation presents excellent, important contributions of many researchers from around the globe, including those of the author and his co-workers.

Contents:
Column Configurations
Operation
Modelling and Simulation
Dynamic Optimisation
Multiperiod Operation Optimisation
Design and Operation Optimisation
Off-Cut Recycle
Batch Reactive Distillation (Bread)
Batch Extractive Distillation (Bed)
Unconventional Batch Distillation
Application of Neural Networks in Batch Distillation
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6. Special Distillation Processes
By Zhigang Lei, Biaohua Chen, Zhongwei Ding,
By Zhigang Lei, Biaohua Chen, Zhongwei Ding,
Publisher: Elsevier Science
Number Of Pages: 370
Publication Date: 2005-03-24
Sales Rank: 3353571
ISBN / ASIN:
🔒 Bấm Cảm ơn hoặc Trả lời để xem SĐT/Liên hệEAN: 9780444516480
Binding: Hardcover
Manufacturer: Elsevier Science
Studio: Elsevier Science
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Book Description:
Special distillation processes are required for separation of mixtures close to boiling point or for forming azeotrope mixtures into their pure components. In Special Distillation Processes, the authors focus on latest developments in the field, such as separation methods that may prove useful for solving problems encountered during research. Topics include extraction, membrane and adsorption distillation involving the separation principle, process design and experimental techniques. The relationship between the processes and the techniques are also presented. Comprehensive and easy-to-read, this book provides key information needed to understand the processes and is a valuable reference source for chemical engineers as well as students wishing to branch out in chemical engineering.
* The only comprehensive book available on special distillation processes
* Contains a thorough introduction to recent developments in the field
* A valuable reference for students and engineers in chemical engineering
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Table of Contents
Ch. 1 Thermodynamic fundamentals 1
Ch. 2 Extractive distillation 59
Ch. 3 Azeotropic distillation 145
Ch. 4 Catalytic distillation 178
Ch. 5 Adsorption distillation 222
Ch. 6 Membrane distillation 241
Ch. 7 Pressure-swing distillation 320
Ch. 8 Other distillation techniques 328
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Kai Sundmacher (Editor), Achim Kienle (Editor), \"Reactive Distillation: Status and Future Directions\"
Wiley-VCH | ISBN 3527305793 | 2003 Year | PDF | 4,2 Mb | 308 Pages
“ In a reactive distillation column, both the chemical conversion and the distillative separation of the product mixture are carried out simultaneously. Through this integrative strategy, chemical equilibrium limitations can be overcome, higher selectivities can be achieved and heat of reaction can be directly used for distillation. Increased process efficiency and reduction of investments and operational costs are the direct results of this approach. Highly renowned international experts from both industry and academia review the state-of-the-art and the future directions in application, design, analysis and control of Reactive Distillation processes. Part I surveys various industrial applications and covers both established large scale processes as well as new chemical reaction schemes with high future potential. Part II provide the vital details for analysis of reactive phase equilibria, and discusses the importance of chemical reaction kinetics, while Part III focuses on identifying feasible column configurations and designing their internal structure. Analysis and control of the complex dynamic and steady-state behavior of reactive distillation processes are described in Part IV. Reactive Distillation - a very promising alternative to conventional reaction-distillation flow schemes.
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